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1-3 Dice & Fill Composites

1-3 Dice & Fill Composites

Smart Material manufactures 1-3 composites using the commonly used Dice & Fill method.

1-3 Dice & Fill Composites specifications

  •   Frequencies 500kHz to 12 MHz
  •   PZT Navy type I,II, III and VI
  •   Fill Factors 25% to 75%
  •   Single Crystal PMN-PT
  •   Maximun dimensions 8cm by 8cm, larger and curved on request
  •   Various epoxy and polyurethane interstitial materials available.
  •   Operational temperatures up to 135℃
  •   Available with Gold, Copper-Tin electrodes

1-3 Dice & Fill Composites

Smart Material manufactures 1-3 composites using the standard Dice & Fill method, which is the current industry standard for frequencies greater than 500kHz.

1-3 Dice & Fill piezo composites are prepared by dicing a piezoceramic plate into an orthogonal array and cutting 80%-90% of the plate thickness. The pitch (distance between rods) must be very small, typically near 100µm at 5 MHz resonance frequency to avoid lateral modes and grating lobes.

The kerfs or trenches are filled with epoxy or other polymer material. After the interstitial material has cured the uncut side of the ceramic is grinded down to the rod structure and the thickness is adjusted to the desired resonance frequency. This yields a regular pixel or rod distribution required for phased array ultrasound transducers.

1-3 D&F Composite product specifications and selections

Resonance Frequencies 500kHZ up to 15MHz                  
 Frequency   Pixel Size Fill Factor Dimensions mm²  Availability
500kHz - 1MHz 400 - 800µm 25% - 75% max. 75 x 75 Request
1MHz - 2MHz 150 - 350µm 25% - 75% max. 75 x 75 Request
2MHz - 6MHz 55 - 200µm 25% - 75% max. 75 x 75 Request
6MHz - 8MHz 75 - 100µm 35% - 65% max. 35 x 35 Request
8MHz - 10MHz 40 - 75µm 50% - 60% max. 35 x 35 Request
10MHz - 15MHz 15 - 35µm 50% - 60% max. 35 x 35 Request
Frequency Tolerances
± 10% typical
± 5% on request
Fill Factors 25% up to 75%
Fill Factor Frequency Availability
25% to 75% 500kHz to 6MHz Request
35% to 65% 6MHz to 8MHz Request
40% to 65% 8MHz to 10MHz Request
Frequency Tolerances
5% typical
PZT Materials PZT Navy Type I, II, III, VI Single Crystal PMN-PT
PZT Material Di-electric Constant      Frequency Availability
PZT Navy Type I, SP4 1200 - 1300 500kHz to 8MHz Request
PZT Navy Type II, 5A 1850 - 2000 500kHz to 10MHz Request
PZT Navy Type III, PZT8 ~ 1050 500kHz to 8MHz Request
PZT Navy Type VI, 5H 3200 - 6200 500kHz to 10MHz Request
Single Crystal PMN-PT 4000 - 7500 2MHz to 10MHz Request
Acoustic Impedance 8.5 MRayl to 26 MRayl
Typical Fill Factors Acoustic Impedance MRayl      
25% 8.5 MRayl
35% 12 MRayl
50% 17 MRayl
65% 22 MRayl
75% 25-26 MRayl
Available Electrodes CuSn (Copper with Tin flash layer) Au (Gold)
Typical Fill Factors Acoustic Impedance MRayl Electrode thickness
CuSn 500kHz to 8MHz ~ 1.5µm
Au 4MHz to 10MHz ~ 0.8µm
Dimensions Max. 75mm by 75mm, various round diameters
Maximum Dimensions Frequency Availability
75mm by 75mm 500kHz to 6MHz Request
35mm by 35mm 6MHz to 8MHz Request
30mm by 30mm 8MHz to 10MHz Request
Mechanical Tolerances:
< 6mm ± 0.1mm
< 30mm ± 0.2mm
> 30mm ± 0.3mm
Available Diameters
∅ in mm ∅ in inch    ∅ in mm    ∅ in inch   
3.18 mm 0.125" 12.70 mm 0.500"
5.12 mm 0.202" 14.20 mm 0.559"
5.18 mm 0.204" 15.90 mm 0.626"
5.68 mm 0.224" 17.50 mm 0.689"
6.00 mm 0.236" 18.00 mm 0.709"
6.50 mm 0.256" 19.05 mm 0.750"
8.20 mm 0.323" 20.00 mm 0.787"
9.00 mm 0.354" 24.00 mm 0.945"
9.50 mm 0.374" 25.40 mm 1"
10.00 mm 0.394" 30.00 mm 1.181"
10.20 mm 0.402" 35.00 mm 1.378"
12.00 mm 0.472" 37.7 mm 1.48"
Coupling Coefficient kt 0.61 to 0.68 for standard PZT materials, > 0.75 for single Crystal
Operational Temperatures Typical 95°C, 135°C on request
Interstitial Materials Various Epoxy systems

Typical Ultrasound Applications for 1-3 D&F Composites

  •   NDT,Non-Destructive Testing
  •   Medical Ultrasound
  •   Flow Control and Measurement
  •   NDT phased array transducer

Compared with the Arrange & Fill production method for our 1-3 random and regular fiber composites, the Dice & Fill method is generally more expensive than similar 1-3 fiber composites due to additional production steps and scalability for volume quantities

Smart Material typically manufactures Dice & Fill standard composites for frequencies between 500kHz and 15MHz with maximum sizes of 75mm by 75mm. Available fill factors range from 25% up to 75% and available PZT materials, for example Navy Type I, Type II (standard), Type III and Type VI (standard). Single crystal materials, i.e. PMN-PT are also available on request.

Smart Material offers various standard epoxy and polyurethane systems as the interstitial material, often called filler. The available filler materials allow for operational temperatures between 95°C and 135°C. Smart Material's machining equipment and capacities also allow the manufacturing of curved 1-3 Dice & Fill piezo composites as well as complex array structures and interconnects.

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